Направления и достижения

Основные направления научной группы

• микроэкстракция органических и неорганических веществ в эвтектические растворители;
• мицеллярная микроэкстракция лекарственных веществ;
• хроматографические методы анализа пищевых продуктов и биологических проб;
• проточные методы анализа;
• хемилюминесцентный скрининг анализ;
• стандартные образцы состава и свойств веществ.

Основные достижения научной группы

Булатов А.В.

• Медаль Российской Академии Наук (2006 г.)
• Лауреат премии Научного Совета по аналитической химии Российской Академии Наук (2008 г.)
• FIA Award for Younger Researcher (The Japanese Association for Flow Injection Analysis) (2014 г.)
• Премия Правительства Санкт-Петербурга в области научно-педагогической деятельности (2014)
• Премия Правительства Санкт-Петербурга в области научно-педагогической деятельности (2015)
• Член научного комитета международной конференции по проточно-инжекционному анализу (The International Conference on Flow Injection Analysis and Related Techniques);
• Член редакционной коллегии журнала Talanta

Вах К.С.

• Лауреат премии Научного Совета по аналитической химии Российской Академии Наук (2018 г.)

Тимофеева И.И.

• Лауреат премии Научного Совета по аналитической химии Российской Академии Наук (2018 г.)
• FIA Award for Younger Researcher (The Japanese Association for Flow Injection Analysis) (2019 г.)

Шишов А.Ю.

• Медаль Российской Академии Наук (2013 г.)
• Лауреат премии Научного Совета по аналитической химии Российской Академии Наук (2021 г.)

Публикации за 3 года

2021 год

1. ​A. Shishov, A. Gerasimov, A. Bulatov. Deep eutectic solvents based on carboxylic acids for metals separation from plant samples: Elemental analysis by ICP-OES. Food Chemistry. 2021. Vol. 366. 130634. DOI: 10.1016/j.foodchem.2021.130634
2. C. Vakh, K. Malkova, E. Syukkalova, N. Bobrysheva, M. Voznesenskiy, A. Bulatov, O. Osmolovskaya. Chemical and computational strategy for design of “switchable” sorbent based on hydroxyapatite nanoparticles for dispersive micro-solid phase extraction of tetracyclines. Journal of Hazardous Materials. 2021. Vol. 419. 126504. DOI: 10.1016/j.jhazmat.2021.126504
3. M. Kochetkova, I. Timofeeva, A. Bulatov. A derivatization and microextraction procedure with organic phase solidification on a paper template: Spectrofluorometric determination of formaldehyde in milk. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 2021. Vol. 263. 120160. DOI: 10.1016/j.saa.2021.120160
4. A. Pochivalov, K. Cherkashina, A. Shishov, A. Bulatov. Microextraction of sulfonamides from milk samples based on hydrophobic deep eutectic solvent formation by pH adjusting. Journal of Molecular Liquids. 2021. Vol. 339. 116827. DOI: 10.1016/j.molliq.2021.116827
5. F. Shakirova, A. Shishov, A. Bulatov. Automated liquid-liquid microextraction and determination of sulfonamides in urine samples based on Schiff bases formation in natural deep eutectic solvent media. Talanta. 2021. Vol. 234. 122660. DOI: 10.1016/j.talanta.2021.122660
6. K. Cherkashina, A. Pochivalov, V. Simonova, F. Shakirova, A. Shishov, A. Bulatov. A synergistic effect of hydrophobic deep eutectic solvents based on terpenoids and carboxylic acids for tetracycline microextraction. Analyst. 2021. Vol. 146. 3449. DOI: 10.1039/D1AN00096A
7. P. Pidenko, C. Vakh, A. Shishov, J. Skibina, N. Burmistrova, A. Bulatov. Microstructured Optical Fibers Sensor Modified by Deep Eutectic Solvent: Liquid-phase Microextraction and Detection in One Analytical Device. Talanta. 2021. Vol. 232. 122305. DOI: 10.1016/j.talanta.2021.122305
8. I. Timofeeva, P. Davletbaeva, A. Moskvin, A. Bulatov. p-Dimethylaminobenzaldehyde-based chemosensor for on-site sensing of ammonia precursor in concrete. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 2021. Vol. 253. 119556. DOI: 10.1016/j.saa.2021.119556
9. C. Vakh, G. Likanov, A. Bulatov. Stir flat sheet membrane liquid phase microextraction for the selective chemiluminescence determination of ofloxacin and fleroxacin in human urine. Microchemical Journal. 2021. Vol. 163. 105913. DOI: 10.1016/j.microc.2020.105913

2020 год

1. К. Черкашина, А. Сумина, К. Вах, А. Булатов. Жидкостная микроэкстракция тетрациклинов из биологических жидкостей для их последующего определения методом высокоэффективной жидкостной хроматографии с УФ-детектированием. Журнал Аналитической химии. 2020. Т. 75(11). С. 1014. DOI: 10.31857/S004445022009007
2. I. Timofeeva, K. Stepanova, A. Bulatov. In-a-syringe surfactant-assisted dispersive liquid-liquid microextraction of polycyclic aromatic hydrocarbons in supramolecular solvent from tea infusion. Talanta. 2021. Vol. 224. 121888. DOI: 10.1016/j.talanta.2020.121888
3. A. Shishov, N. Volodina, S. Gagarinova, V. Shilovskikh, A. Bulatov. A rotating disk sorptive extraction based on hydrophilic deep eutectic solvent formation. Analytica Chimica Acta. Vol. 1141. 163. DOI: 10.1016/j.aca.2020.10.020
4. I. Timofeeva, K. Stepanova, A. Shishov, L. Nugbienyo, L. Moskvin, A. Bulatov. Fluoroquinolones extraction from meat samples based on deep eutectic solvent formation.  Journal of Food Composition and Analysis. 2020. Vol. 93. 103589. DOI: 10.1016/j.jfca.2020.103589
5. A. Shishov, A. Gorbunov, E. Baranovskii, A. Bulatov, Microextraction of sulfonamides from chicken meat samples in three-component deep eutectic solvent. Microchemical Journal. 2020. Vol. 158. 105274. DOI: 10.1016/j.microc.2020.105274
6. A. Shishov, A. Pochivalov, L. Nugbienyo, V. Andruch, A. Bulatov. Deep eutectic solvents are not only effective extractants. Trends in Analytical Chemistry. 2020. Vol. 129. 115956. DOI: 10.1016/j.trac.2020.115956
7. I. Timofeeva, M. Alikina, M. Osmolowsky, O. Osmolovskaya, A. Bulatov. Magnetic headspace adsorptive microextraction using Fe₃O₄@Cr(OH)₃ nanoparticles for effective determination of volatile phenols. New Journal of Chemistry. 2020. Vol. 44. 8778. DOI: 10.1039/D0NJ00854K
8. C. Vakh, A. Kuzmin, A. Sadetskaya, P. Bogdanova, M. Voznesenskiy, O. Osmolovskaya, A.Bulatov. Cobalt-doped hydroxyapatite nanoparticles as a new eco-friendly catalyst of luminol-H2O2 based chemiluminescence reaction: study of key factors, improvement the activity and analytical application. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 2020. Vol. 237. 118382. DOI: 10.1016/j.saa.2020.118382
9. P. Bogdanova, A. Pochivalov, C. Vakh, A. Bulatov. Supramolecular solvents formation in aqueous solutions containing primary amine and monoterpenoid compound: Liquid phase microextraction of sulfonamides. Talanta. 2020. Vol. 216. 120992 DOI: 10.1016/j.talanta.2020.120992
10. A. Shishov, A. Gerasimov, D. Nechaeva, N. Volodina, E. Bessonova, A. Bulatov. An effervescence-assisted dispersive liquid-liquid microextraction based on deep eutectic solvent decomposition: Determination of ketoprofen and diclofenac in liver. 2020. Microchemical Journal. Vol. 156. 104837. DOI: 10.1016/j.microc.2020.104837
11. D. Kanashina, A. Pochivalov, I. Timofeeva, A. Bulatov. Mixed surfactant systems based on primary amine and medium-chain fatty acid: Micelle-mediated microextraction of pesticides followed by the GC–MS determination. Journal of Molecular Liquids. 2020. Vol. 306. 112906. DOI: 10.1016/j.molliq.2020.112906
12. K. Cherkashina, M. Voznesenskiy, O. Osmolovskaya, C. Vakh, A. Bulatov. Effect of surfactant coating of Fe3O4 nanoparticles on magnetic dispersive micro-solid phase extraction of tetracyclines from human serum. Talanta. 2020. Vol. 214. 120861. DOI: 10.1016/j.talanta.2020.120861.
13. A. Shishov, S. Gagarionova, A. Bulatov. Deep eutectic mixture membrane-based microextraction: HPLC-FLD determination of phenols in smoked food samples. Food Chemistry. 2020. Vol. 314. 126097. DOI: 10.1016/j.foodchem.2019.126097

2019 год

1. S. Lebedinets, C. Vakh, K. Cherkashina, A. Pochivalov, L. Moskvin, A. Bulatov. Stir membrane liquid phase microextraction of tetracyclines using switchable hydrophilicity solvents followed by high-performance liquid chromatography. Journal of Chromatography A. 2019. DOI: 10.1016/j.chroma.2019.460743.
2. A. Shishov, A. Gorbunov, L. Moskvin, A. Bulatov. Decomposition of deep eutectic solvents based on choline chloride and phenol in aqueous phase. Journal of Molecular Liquids. 2019. DOI: 10.1016/j.molliq.2019.112380.
3. A. Pochivalov, C. Vakh, S. Garmonov, L. Moskvin, A. Bulatov. An automated in-syringe switchable hydrophilicity solvent-based microextraction. Talanta. 2019. DOI: 10.1016/j.talanta.2019.120587.
4. С. Vakh, I. Timofeeva, A. Bulatov. Automation of Microextraction Preconcentration Methods Based on Stepwise Injection Analysis Journal of Analytical Chemistry. 2019. DOI: 10.1134/S106193481911011X.
5. A.Shishov, E.Stolarova, L.Moskvin, A.Bulatov. Reversed-phase chromatomembrane extraction as a novel approach for automated sample pretreatment: Anions determination in biodiesel by ion chromatography with conductivity detection. Analytica Chimica Acta. 2019. DOI:10.1016/j.aca.2019.08.031.
6. A.Shishov, P.Terno, L.Moskvin, A.Bulatov. In-syringe dispersive liquid-liquid microextraction using deep eutectic solvent as disperser: Determination of chromium (VI) in beverages. Talanta. 2020. DOI: 10.1016/j.talanta.2019.120209.
7. A.Shishov, I.Trufanov, D. Nechaeva, A. Bulatov. A reversed-phase air-assisted dispersive liquid-liquid microextraction coupled with colorimetric paper-based analytical device for the determination of glycerol, calcium and magnesium in biodiesel samples. Microchemical Journal. 2019. DOI:10.1016/j.microc.2019.104134.
8. А.В. Булатов, А.Ю. Шишов, Л.Н. Москвин. Концепция равновесных проточных методов. Циклический инжекционный анализ и его аналитические возможности. Журнал аналитической химии. 2019. Т.74. №10. С. 774-783.
9. A. Shishov, D. Nechaeva, A. Bulatov. HPLC-MS/MS determination of non-steroidal anti-inflammatory drugs in bovine milk based on simultaneous deep eutectic solvents formation and its solidification. Microchemical Journal. 2019. DOI: 10.1016/j.microc.2019.104080.
10. K. Cherkashina, S. Lebedinets, A. Pochivalov, A. Lezov, C. Vakh, A. Bulatov. Homogeneous liquid-liquid microextraction based on primary amine phase separation: a novel approach for sample pretreatment. Analytica Chimica Acta. 2019. DOI: 10.1016/j.aca.2019.04.070.
11. I.Timofeeva, D. Kanashina, K. Stepanova, A. Bulatov. A simple and highly-available microextraction of benzoic and sorbic acids in beverages and soy sauce samples for high performance liquid chromatography with ultraviolet detection. Journal of Chromatography A. 2019. DOI: 10.1016/j.chroma.2018.12.030.
12. A. Shishov, R. Chromá, C. Vakh, J. Kuchár, A. Simon, V. Andruch, A. Bulatov. In situ decomposition of deep eutectic solvent as a novel approach in liquid-liquid microextraction. Analytica Chimica Acta. 2019. DOI:10.1016/J.ACA.2019.03.038.
13. A. Bulatov, L. Moskvin, O. Rodinkov, S. Ermakov, Department of Analytical Chemistry of Saint Petersburg State University Celebrates One Hundred and Fifty Years Anniversary: International Year of the Periodic Table of Chemical Elements. Talanta. 2019. DOI: 10.1016/j.talanta.2019.03.081.
14. Christina Vakh, Marcel Alaboud, Sofya Lebedinets, Andrey Bulatov. A rotating cotton-based disk packed with a cation-exchange resin: Separation of ofloxacin from biological fluids followed by chemiluminescence determination. Talanta. 2019. V. 196. P. 117-123. DOI: 10.1016/j.talanta.2018.12.024.
15. Irina Timofeeva, Mariya Alikina, Anna Vlasova, Mikhail Osmolowsky, Mikhail Voznesenskiy, Olga Volina, Leonid Moskvin, Olga Osmolovskaya, Andrey Bulatov. Fe3O4-based composite magnetic nanoparticles for volatile compound sorption in gas phase: determination of selenium (IV). Analyst. 2019. V. 144. P. 152 - 156. DOI: 10.1039/C8AN01894D.